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A tube furnace is often the most economical way to heat a small sample, allowing rapid temperature changes and excellent temperature uniformity.
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The furnace must be operated under high vacuum (less than 10-4 Torr) KNOW YOUR SAMPLE! Researchers must verify that their sample will maintain low vapor pressure (<10E-5 Torr) and not react with its surroundings at high temperature. Safety Interlocks The furnace requires high vacuum and sufficient water flow for safe operation.
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GAS-FIRED GRAVITY DIRECT VENT WALL FURNACE GAS-FIRED GRAVITY DIRECT VENT WALL FURNACE INSTALLATION AND OPERATION dents, corrosion or discolouring caused by excessive heat, abrasive and chemical cleaners nor chipping on porcelain enamel The bill of sale or copy will be required together with a serial number and a model Access Document
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Porcelain, per se, isn't a very good refractory: the difference between it, and any other common ceramic like stoneware, is its very low porosity and very high glass content. The only reason porcelain doesn't melt to globs during firing is the strategic use of alumina, which remains solid as a crystalline mullite network.